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KMID : 0366119730010010051
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Korean Journal of Applied Microbiology & Bioengineering
1973 Volume.1 No. 1 p.51 ~ p.57
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Studies on Derivatives of 2, 2´-Methylene bis (3, 4, 6-trichloroacetoxy benzene)
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Abstract
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2, 2´-Methylene bis (3, 4, 6-trichloroacetoxy benzene) had been synthesiged from Hexachlorophene.
The eleven new derivatives -(2, 2´Methylene bis [3, 4, 6 -trichloro o-(β-anilinopropionoxy) benzene: m. p 173∼4℃, C₃₁H₂₄N₂O₄Cl_(6), 2,2´ Methylene bis [3, 4, 6-trihcloro (β-Cyclohexylami nopropionoxy) benzene]: M. P. 187∼8℃, C₃₁H_(36)N₂O₄Cl_(6), 2, 2´-Methylene bis [3, 4, 6- tricbloro (β-phenyl hydrazinopropionoxy) benzene]; M. P. 151∼3℃, C₃₃H_(28)N₂O₄Cl_(6), 2, 2´ Methylene bis [3, 4, 6-trichloro (β-o-toluidinopropionoxy) benzene]; M. P. 172∼3℃, C₃₃H_(28)N₂O₄Cl_(6), 2,2´Methylene bis [3, 4, 6-trichloro (β-p-todudinopropionoxy) bennzene]; 153∼4℃, C₃₃H_(28)N₃O₄Cl_(6), 2, 2´-Methylene bis [3, 4, 6-trichloro (β-o-chloro anilinopropionoxy) benzene]; 170∼2℃, C₃₁H_(27)N₂Cl_(8)O₄, 2, 2´-Methylene bis [3, 4, 6-trichloro (β-p-sulfamili noprooionoxy)benzene]; M. P. 310∼5℃, C₃₁H₂₄N₃S₂O_(10)Cl_(6), 2, 2´-Methylene bis [3, 4, 6-trichloro (β-pipridinopropionoxy) benzene]; M. P 168∼2℃, C_(29)H₃₂N₂O₄Cl_(6), 2, 2´-Methylene bis [3, 4, 6-trichloro (β-morpholinopropionoxy) benzene]; M. P. 226∼8℃, C_(27)H₂₃N₂O_(6)Cl_(6) 2, 2´-Methylene bis (3, 4, 6 trichloro (β-2-amino pyridino propionoxy) benzene]; M. P. 145∼6℃, C_(29)H₂₂N₄O₄Cl_(5)―were synthesized by Mann cbs reaction as potential antimicrobial agents and their antimicrobial activity were tested against Bacillus subtilis, Pseudomonas ovals, Escherichia coli, Staphylococcus aureus,
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